SOP for Preparation of Carbon-Based Nanomaterials

Standard Operating Procedure for Preparation of Carbon-Based Nanomaterials

1) Purpose

This SOP outlines the procedure for preparing carbon-based nanomaterials, such as graphene, carbon nanotubes, and fullerenes, which are used in various applications including drug delivery, electronics, and energy storage.

2) Scope

This SOP applies to personnel involved in the synthesis and characterization of carbon-based nanomaterials for research or industrial purposes.

3) Responsibilities

Operators: Responsible for synthesizing carbon-based nanomaterials and performing quality control tests.
QA: Ensures that the nanomaterials meet the required specifications for purity, particle size, and structure.

4) Procedure

4.1 Synthesis of Carbon Nanomaterials

4.1.1 Chemical Vapor Deposition (CVD) Method

4.1.1.1 Use the CVD method to synthesize graphene or carbon nanotubes by depositing carbon atoms onto a substrate through the thermal decomposition of a carbon source (e.g., methane).

4.1.2 Arc Discharge Method

4.1.2.1 Alternatively, use the arc discharge method to synthesize fullerenes or multi-walled carbon nanotubes by vaporizing carbon electrodes in an inert atmosphere.

4.2 Purification and Characterization

4.2.1 Purification

4.2.1.1 Purify the synthesized carbon nanomaterials using acid treatments or thermal oxidation to remove any impurities or catalyst residues.

4.2.2 Characterization

4.2.2.1 Characterize the nanomaterials using techniques such as scanning electron microscopy (SEM), transmission electron microscopy (TEM), and Raman spectroscopy to determine their structure, purity, and size.

4.3 Stability and Storage

4.3.1 Stability Testing

4.3.1.1

Conduct stability studies under different environmental conditions (e.g., temperature, humidity) to assess the long-term stability of the nanomaterials.

4.3.2 Storage Conditions

4.3.2.1 Store the carbon-based nanomaterials in sealed, dry containers at room temperature to prevent oxidation or degradation.

5) Abbreviations, if any

CVD: Chemical Vapor Deposition
SEM: Scanning Electron Microscopy
TEM: Transmission Electron Microscopy

6) Documents, if any

Carbon Nanomaterial Synthesis Logbook

7) References, if any

Protocols for carbon-based nanomaterial synthesis and characterization

8) SOP Version

Version 1.0

Annexure

Carbon Nanomaterial Synthesis Logbook Template


  
    Date
    Batch Number
    Synthesis Method
    Purity Level
    Particle Size
    Operator Initials
    QA Initials
  
  
    DD/MM/YYYY
    Batch Number
    CVD/Arc Discharge
    Purity (%)
    Size in nm
    Operator Name
    QA Name

Date	Batch Number	Synthesis Method	Purity Level	Particle Size	Operator Initials	QA Initials
DD/MM/YYYY	Batch Number	CVD/Arc Discharge	Purity (%)	Size in nm	Operator Name	QA Name